The Chinese University of Hong Kong
Department of Chemistry
Basic Laboratory Techniques
[b]Heating and Refluxing
Simple Filtration - Filter Cone
Simple Filtration -
Prepare the Fluted Filter Paper
Simple Filtration - Fluted Filter Paper
Vacuum Filtration (Suction Filtration)
Recrystallization
Simple Distillation
Extraction
Drying an Organic Solution
Fractional Distillation
Vacuum Distillation
Use of Rotary Evaporator
[/b]
http://rapidshare.com/files/75670415/BasicLaboratoryTechniques_www.forumakademi.org.rar
Chromatographic Techniques
[b]Thin Layer Chromatography (TLC)
Column Chromatography 1:
Preparing the Column
Column Chromatography 3:
Eluting the Column and Fractions Collecting
Gas Chromatography (GC) -
Auto Sample Injection
Gas Chromatography (GC) -
Manual Sample Injection
High Performance Liquid Chromatography (HPLC) -
Auto Sample Injection
High Performance Liquid Chromatography (HPLC) -
Manual Sample Injection
[/b]
http://rapidshare.com/files/75649459/GasChromatography_www.forumakademi.org.rar
Spectroscopic Analytical Techniques
[b]Ultraviolet-Visible Spectrophotometry (UV-Vis)
Infrared Spectrometry (IR) - Liquid Sample
Infrared Spectrometry (IR) - Solid Sample
Nuclear Magnetic Resonance Spectrometry (NMR)
[/b]
http://rapidshare.com/files/75651618/Spectroscopic_www.forumakademi.org.rar
Quantitative Analysis
[b]Weighing
Use of Volumetric Flask
Pipetting
Volumetric Titration
[/b]
http://rapidshare.com/files/75654782/QuantitativeAnalysis_www.forumakademi.org.rar
Miscellaneous Instrumental Techniques
[b]
pH Measurement Using Glass Electrode
Magnetic Susceptibility Balance (MSB)
Polarimeter
Voltammetric Analyzer
Differential Scanning Calorimetry
Thermogravimetric Analysis
[/b]
http://rapidshare.com/files/75658123/InstrumentalTechniques_www.forumakademi.org.rar
Handling of Air Sensitive Compounds
[b]The Schlenk-Line Technique: Part 1
The Schlenk-Line Technique: Part 2
The Schlenk-Line Technique: Part 3
The Schlenk-Line Technique: Part 4
Use of The Dry Box: Part 1
Use of The Dry Box: Part 2
Use of The Dry Box: Part 3
[/b]
http://rapidshare.com/files/75661363/AirSensitiveCompounds_www.forumakademi.org.rar